P Premedalltheway Member 10+ Year Member 5+ Year Member 15+ Year Member Joined Oct 8, 2004 Messages 44 Reaction score 0 Oct 8, 2004 #1 Members do not see this ad. why is it necessary to dry the recrystallized compound before taking a melting poiint?
Members do not see this ad. why is it necessary to dry the recrystallized compound before taking a melting poiint?
Fermata Hold me. Verified Member Physician 15+ Year Member Joined Dec 11, 2003 Messages 6,617 Reaction score 14 Oct 8, 2004 #2 Premedalltheway said: why is it necessary to dry the recrystallized compound before taking a melting poiint? Click to expand... So you can see it MELT. 😀
Premedalltheway said: why is it necessary to dry the recrystallized compound before taking a melting poiint? Click to expand... So you can see it MELT. 😀
Fermata Hold me. Verified Member Physician 15+ Year Member Joined Dec 11, 2003 Messages 6,617 Reaction score 14 Oct 8, 2004 #3 Just kidding. You let it dry because the water/solvent can greatly affect the MP of the compound. You want as pure a sample as possible.
Just kidding. You let it dry because the water/solvent can greatly affect the MP of the compound. You want as pure a sample as possible.
Fermata Hold me. Verified Member Physician 15+ Year Member Joined Dec 11, 2003 Messages 6,617 Reaction score 14 Oct 8, 2004 #4 As a side note.......one time we had to rush a recrystallization where we didn't have time to let the recystallized compound dry.... We got a yield of about 200% and a ridiculously wrong MP measurement. LOL.
As a side note.......one time we had to rush a recrystallization where we didn't have time to let the recystallized compound dry.... We got a yield of about 200% and a ridiculously wrong MP measurement. LOL.